Documents / Document

ORNL Synopsis: Analysis of a Metallic Specimen

All-domain Anomaly Resolution Office · 2024-07 · 10 pages · text from the file's own layer

No summary written yet.

Synopsis: Analysis of a Metallic Specimen4
Finally, based on the postulated hypothetical uses of bismuth, the dielectric properties necessary for bismuth to
function as a waveguide would have been disrupted in this material because the bismuth in the specimen is co-
located and mixed with lead (Figures 3 and 5). Based on these findings ORNL determined that this material is highly
unlikely to have ever functioned as a bismuth-based terahertz waveguide.
5 μm
(a)
5 nm-1
(b)
5 μm 5 nm-1
γ =3.0
Bi2O3
Bi
(c) (d)
Figure 4: (a) TEM micrograph of a single-crystalline region from the bulk of the sample; structural defects are visible at
this level of resolution (this figure is showing an area that represents just 2 to 3 pixels of the area shown in Figure 3). The
vertical lines at the bottom are a focused ion beam preparation artifact. (b) Selected area electron diffraction pattern
(SAEDP) from the region in (a), indexed to the standard Mg structure. (c) A low-magnification montage TEM micrograph
of an area showing a dense bismuth-rich layer (dark central band). (d) A SAEDP from a bismuth-rich band. The electron
diffraction pattern (with image processing γ=3.0) from the bismuth-rich region is shown in the white rings. Both bismuth
(Bi, yellow) and Bi2O3 (red) calculated ring patterns are shown for comparison; Bi is a slightly better match. The diffraction
indicates that the bismuth layer is nanocrystalline and highly defective.

Not linked to a story yet.

About this file

Document, cited by the archive. The PDF is mirrored here; the original link is above. 10 pages are in the text index: search them above, or from the library's search.